ENCYCLOPEDIA OF RADIO ELECTRONICS AND ELECTRICAL ENGINEERING Manufacture of organic oLED LEDs. Encyclopedia of radio electronics and electrical engineering Encyclopedia of radio electronics and electrical engineering / Ham Radio Technologies What is an organic LED? Organic Light-Emitting Diode (oLED) - an organic light-emitting diode, made from organic compounds capable of emitting light when a current is passed. In this article, we will look at how to make organic oLEDs in a home laboratory with our own hands. The coordination complex between the transparent tin oxide electrode and the active metal electrode emits light when an external voltage is applied. Coating too thin a layer of [Ru(bipyridine)3](BF4)2-polyvinyl alcohol will result in a short circuit and no light emission; a coating that is too thick will have too high an electrical resistance and will also result in no radiation. Determine the conductive side of the tin oxide coated glass sample by measuring the resistance with a tester. The final resistance of the conductive side should be 20-30 ohms. Use double-sided adhesive tape to secure the indium tin oxide coated glass, conductive side out, to a fan at up to 2500 rpm. Using a cotton swab, apply a solution of [Ru(bipyridine)3](BF4)2- polyvinyl alcohol on the central part of the glass. Rotate the sample at 2500 rpm for 30-60 s, use a protective shield to prevent splashing. Repeat the application 3-4 times, leaving the edges uncovered. Instead of the preferred rotation coating method, you can use double-sided adhesive tape to attach the indium tin oxide coated glass with the conductive side out to the table surface. Apply a very thin layer of [Ru(bipyridine)3](BF4)2-polyvinyl alcohol on glass. Evaporate the liquid with a heat gun or hair dryer. Repeat the application 3-4 times, leaving the edges uncovered. Make a stencil. To do this, glue a piece of electrical tape to aluminum foil and pierce a hole in it with a diameter of approximately 3 mm. Dry the glass with a hair dryer for at least a minute to remove any liquid remaining on the film. The first reason for the failure in the manufacture of organic light emitting diodes oLED is due to insufficient drying of the polymer layer before applying the active metal layer. Using a cotton swab, apply a liquid alloy of gallium and indium (active metal electrode) through the stencil. Eutectic mixture of 75,5% gallium and 24,5% indium liquid at temperatures above 16,5оC. Connect the positive lead of the 4,5V power supply to tin oxide coated glass (not polymer coated). Carefully connect the negative lead to the gallium-indium alloy. In a humid environment, the service life is significantly reduced. View from the uncoated side of the glass. Or watch in the dark. Is this section a diode? What happens if the polarity of the supplied voltage is reversed? Materials Ready-made solutions for various preparations: Place approximately 0,30 g of PVA (polyvinyl alcohol, Aldrich, 36,316-2, average molecular weight 124 - 000) and 186 ml of water in a 000 ml beaker. To dissolve the PVA, cover the beaker loosely with plastic and heat in the microwave several times for 10 seconds until completely dissolved. Do not let the solution boil. Dissolve approximately 0,035 g of [Ru(bipyridine)3](BF4)2 (synthesis - see article 2) in 3 ml of polyvinyl alcohol solution. GaIn Eutectic (Eutectic mixture of gallium and indium), Aldrich, 49542-5 Equipment:
Modified by Jason Marmon, George Lisensky, and Wendy deProfetis using the following sources: Frank G. Gao, Allen J. Bard "Semiconductor Organic Light-Emitting Diodes Based on Tris(2,2'-bipyridine)ruthenium(II) Complexes", Journal of American Chemistry Society, 122(30), 7426-7427 (2000); Hanna Sevjan, Sin Muller, Hartmut Rudmann, Michael F. Rabner "The Use of Organic Light-Emitting Electrochemical Thin Film Components in the Study of Materials Science", Journal of Chemical Education, 81(11), 1620 (2004). Publication: cxem.net See other articles Section Ham Radio Technologies. Read and write useful comments on this article. Latest news of science and technology, new electronics: Artificial leather for touch emulation
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